Journal ArticleDOI
Application of commercial microwave ovens to organic synthesis.
TLDR
In this article, commercial microwave ovens have been safely used to dramatically reduce the reaction times (at comparable yield) of Diels-Alder, Claisen, and ene reactions.About:
This article is published in Tetrahedron Letters.The article was published on 1986-01-01. It has received 1028 citations till now. The article focuses on the topics: Microwave oven.read more
Citations
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Journal ArticleDOI
Comparison of Conventional and Microwave Heating for Evaluation of Microwave Effects
Péter Bana,István Greiner +1 more
TL;DR: In this article, a method to eliminate most of the irreproducibility observed in microwave-heated organic transformations by thermal conditioning of the microwave reactor cavity was proposed. But this method is limited to the case of 2-chloropyridine.
Journal ArticleDOI
Rapid augmentation of vertically aligned MoO3 nanorods via microwave irradiation
TL;DR: This work has demonstrated a simple, low cost and swift method to prepare vertically aligned hexagonal MoO3 nanorods on substrates using microwave irradiation, which most interestingly, can be converted to layered α-MoO3 keeping the vertical alignment intact.
Dissertation
Design of targeted photosensitizer-conjugates towards Neuropilin-1 and folate receptors for improving the selectivity of anti-cancer photodynamic therapy
TL;DR: This thesis focuses on improving the selectivity of PS delivery through designing targeted PS agents that bonds with high efficiency to folic acid receptor over-expressed on the surface of many cancer cells.
Journal ArticleDOI
Supported Tetramethylamonium Nitrate/Silicasulfuric Acid as a Useful Reagent for Nitration Aromatic Compounds Under Solvent‐Free Conditions
TL;DR: A variety of aromatic compounds are nitrated to the parent nitro aromatic compounds under solvent-free conditions using supported tetramethylammonium nitrate/silicasulfuric acid as a useful reagent as discussed by the authors.
Dissertation
Bi-layered chromatography matrices for the purification of biological nanoplexes
TL;DR: In this article, the preparation of SEC/IEC supports from commercially available, underivatised base matrices by AGE activation-partial bromination technique via two different approaches; (i) viscosity enhanced-reaction diffusion (VE-RD) and (ii) microwave-assisted reaction diffusion, were studied and optimised.
References
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Journal ArticleDOI
Acceleration of the diels-alder reaction by aluminum chloride
Peter Yates,Philip E. Eaton +1 more
Journal ArticleDOI
Some Reactions of Δ2-Cyclohexenone, Including the Synthesis of Bicyclo(2,2,2)-octanedione-2,6
Journal ArticleDOI
The reaction of anthracene with maleic and fumaric acid and their derivatives and with citraconic anhydride and mesaconic acid.
W. E. Bachmann,L. B. Scott +1 more
TL;DR: The initial precipitate of long dense needles had become contaminated by a small superficial layer of fluffy crystalline balls, apparently containing the saturated dioltrione (XXIV) and after two further recrystallizations from alcohol melted at 23!-238’.
Journal ArticleDOI
Chlorination of organoboranes: synthesis of (z)-vinyl chlorides
TL;DR: Chloration d'(alcene-1yl dihydroxy) boranes et obtention stereoselective de cis-chloro-1 alcenes as mentioned in this paper.