Journal ArticleDOI
Application of commercial microwave ovens to organic synthesis.
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In this article, commercial microwave ovens have been safely used to dramatically reduce the reaction times (at comparable yield) of Diels-Alder, Claisen, and ene reactions.About:
This article is published in Tetrahedron Letters.The article was published on 1986-01-01. It has received 1028 citations till now. The article focuses on the topics: Microwave oven.read more
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Book ChapterDOI
Synthesis of nanomaterials and compounds via microwave irradiation as a greener alternative
TL;DR: In this paper, the authors explore the basis and main features of microwave irradiation focusing on the most common applications in the synthesis of nanomaterials and organic compounds, and present a survey of microwave-based methods for chemical reactions.
Journal ArticleDOI
Microwave Irradiation as a Powerful Tool for the Preparation of n-Type Benzotriazole Semiconductors with Applications in Organic Field-Effect Transistors
Iván Torres-Moya,Alexandra Harbuzaru,Beatriz Donoso,Pilar Prieto,Rocío Ponce Ortiz,Angel Díaz-Ortiz +5 more
TL;DR: In this paper , a complex pyrazinedecorated benzotriazole derivative that is challenging to prepare under conventional conditions has been obtained upon microwave irradiation, thus efficiently improving the process and yields, dramatically decreasing the reaction times and resulting in an environmentally friendly synthetic procedure.
Journal ArticleDOI
Microwave Catalyzed Reaction of H-Dimethylphosphonate with N-(2,3-Epoxypropyl)Phthmide
TL;DR: In this article, the mechanism of formation of the various compounds along with their mass spectral fragmentation behavior is described in a microwave catalyzed reaction of N-(2,3-epoxypropyl)phthalimide with H-dimethylphosphonate for 4 min yielded via free radical processes.
Journal ArticleDOI
Template synthesis and adsorption properties of chitosan salicylal Schiff bases
TL;DR: In this paper, the adsorption capacity and selectivity coefficient of chemically modified chitosan for Cu(II), Fe(III) and Zn(II) were investigated.
References
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Journal ArticleDOI
Acceleration of the diels-alder reaction by aluminum chloride
Peter Yates,Philip E. Eaton +1 more
Journal ArticleDOI
Some Reactions of Δ2-Cyclohexenone, Including the Synthesis of Bicyclo(2,2,2)-octanedione-2,6
Journal ArticleDOI
The reaction of anthracene with maleic and fumaric acid and their derivatives and with citraconic anhydride and mesaconic acid.
W. E. Bachmann,L. B. Scott +1 more
TL;DR: The initial precipitate of long dense needles had become contaminated by a small superficial layer of fluffy crystalline balls, apparently containing the saturated dioltrione (XXIV) and after two further recrystallizations from alcohol melted at 23!-238’.
Journal ArticleDOI
Chlorination of organoboranes: synthesis of (z)-vinyl chlorides
TL;DR: Chloration d'(alcene-1yl dihydroxy) boranes et obtention stereoselective de cis-chloro-1 alcenes as mentioned in this paper.