Journal ArticleDOI
Application of commercial microwave ovens to organic synthesis.
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TLDR
In this article, commercial microwave ovens have been safely used to dramatically reduce the reaction times (at comparable yield) of Diels-Alder, Claisen, and ene reactions.About:
This article is published in Tetrahedron Letters.The article was published on 1986-01-01. It has received 1028 citations till now. The article focuses on the topics: Microwave oven.read more
Citations
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Journal ArticleDOI
Development of a water load for a Ka-band 10 kW continuous-wave gyrotron in an ECR ion source system
Jung-Woo Ok,Seyong Choi,Byoung-Seob Lee,Jang-Hee Yoon,Jin Yong Park,Chang Seouk Shin,Mi-Sook Won,In Seok Hong +7 more
TL;DR: In this article, a water load consisting of an aluminum jacket, a quartz window, and a waveguide was used to absorb up to 10 kW of power at 28 GHz in the continuous wave (CW) mode.
Proceedings ArticleDOI
Microwave-assisted rapid synthesis of ionic liquids
Ming-Chien Hsiao,Tse-Wei Lin +1 more
TL;DR: In this paper, the use of microwave assisted synthesis of ionic liquids can effectively reduce the synthesis time and the yield synthesis in comparison with the traditional reaction, and the best yield was about 49.5%.
Dissertation
Synthesis, Characterization And Biological Evaluation Of Some Metal Complexes With Ligands Containing Cyclic Moieties
TL;DR: In this article, the synthesis and characterization of compounds containing cyclic and heterocyclic moieties, Phthalimide and phenyl amide compounds aiming at search of new candidates to battle with microorganisms.
Journal ArticleDOI
Effect of Oxidizers on Microwave-Assisted Oxidative Degradation of Poly(alkyl acrylates)
A. Marimuthu,Giridhar Madras +1 more
TL;DR: In this paper, the effect of oxidizers on the microwave-assisted oxidative degradation kinetics of poly(alkyl acrylates), namely, poly(methyl acrylate) (PMA), poly(ethyl acrylated) (PEA), and poly(butyl acRYlate)(PBA), was studied.
Organic synthesis - applications in enzymatic studies, catalysis and surface modification
TL;DR: A theory to predict and/or explain the activity of the enzyme on engineered phospholipids, and a novel selective method for functionalizing liposomes, which has not yet been reported in the literature are developed.
References
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Journal ArticleDOI
Acceleration of the diels-alder reaction by aluminum chloride
Peter Yates,Philip E. Eaton +1 more
Journal ArticleDOI
Some Reactions of Δ2-Cyclohexenone, Including the Synthesis of Bicyclo(2,2,2)-octanedione-2,6
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The reaction of anthracene with maleic and fumaric acid and their derivatives and with citraconic anhydride and mesaconic acid.
W. E. Bachmann,L. B. Scott +1 more
TL;DR: The initial precipitate of long dense needles had become contaminated by a small superficial layer of fluffy crystalline balls, apparently containing the saturated dioltrione (XXIV) and after two further recrystallizations from alcohol melted at 23!-238’.
Journal ArticleDOI
Chlorination of organoboranes: synthesis of (z)-vinyl chlorides
TL;DR: Chloration d'(alcene-1yl dihydroxy) boranes et obtention stereoselective de cis-chloro-1 alcenes as mentioned in this paper.