Journal ArticleDOI
Application of commercial microwave ovens to organic synthesis.
TLDR
In this article, commercial microwave ovens have been safely used to dramatically reduce the reaction times (at comparable yield) of Diels-Alder, Claisen, and ene reactions.About:
This article is published in Tetrahedron Letters.The article was published on 1986-01-01. It has received 1028 citations till now. The article focuses on the topics: Microwave oven.read more
Citations
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Solvent-free microwave organic synthesis as an efficient procedure for green chemistry
TL;DR: Les techniques de reactions without solvant sont particulierement adaptees aux conditions de la chimie verte as discussed by the authors, and en resulte des procedes efficaces et propres, avec de notables ameliorations par rapport aux methodes classiques.
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Progress in microwave-assisted synthesis of quantum dots (graphene/carbon/semiconducting) for bioapplications: a review
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Microwave assisted synthesis of pyrroles
TL;DR: The synthesis of pyrroles by reaction of hexane-2,5-dione with primary amines has been shown to occur in less than 2 minutes under microwave activation.
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Highly stable amorphous calcium phosphate porous nanospheres: microwave-assisted rapid synthesis using ATP as phosphorus source and stabilizer, and their application in anticancer drug delivery.
TL;DR: The as-prepared ACP porous nanosphere drug-delivery system with docetaxel shows a high ability to damage tumor cells, thus, is promising for the application in anticancer treatment.
Journal ArticleDOI
Intensification of desorption processes by use of microwaves—An overview of possible applications and industrial perspectives
TL;DR: In this paper, the state of the art regarding the possible intensification of desorption processes by use of microwave irradiation is presented and the most important experimental and modeling results reported in the literature on the laboratory scale as well as on the industrial scale were collected in this paper.
References
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Journal ArticleDOI
Acceleration of the diels-alder reaction by aluminum chloride
Peter Yates,Philip E. Eaton +1 more
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Some Reactions of Δ2-Cyclohexenone, Including the Synthesis of Bicyclo(2,2,2)-octanedione-2,6
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The reaction of anthracene with maleic and fumaric acid and their derivatives and with citraconic anhydride and mesaconic acid.
W. E. Bachmann,L. B. Scott +1 more
TL;DR: The initial precipitate of long dense needles had become contaminated by a small superficial layer of fluffy crystalline balls, apparently containing the saturated dioltrione (XXIV) and after two further recrystallizations from alcohol melted at 23!-238’.
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Chlorination of organoboranes: synthesis of (z)-vinyl chlorides
TL;DR: Chloration d'(alcene-1yl dihydroxy) boranes et obtention stereoselective de cis-chloro-1 alcenes as mentioned in this paper.