Journal ArticleDOI
Application of commercial microwave ovens to organic synthesis.
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In this article, commercial microwave ovens have been safely used to dramatically reduce the reaction times (at comparable yield) of Diels-Alder, Claisen, and ene reactions.About:
This article is published in Tetrahedron Letters.The article was published on 1986-01-01. It has received 1028 citations till now. The article focuses on the topics: Microwave oven.read more
Citations
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Journal ArticleDOI
Process intensification: oxidation of benzyl alcohol using a continuous isothermal reactor under microwave irradiation
TL;DR: In this article, the concept of process intensification has been used to develop a narrow channel reactor that is capable of carrying out reactions under isothermal conditions while being exposed to microwave irradiation.
Journal ArticleDOI
Alumina-mediated cleavage of t-butyldimethylsilyl ethers
TL;DR: In this article, a simple method for the cleavage of t -butyldimethylsilyl ethers is described which occurs on alumina surface under solvent free conditions within 10-15 minutes.
Journal ArticleDOI
Microwave-Assisted Organic Synthesis in Near-Critical Water at 300 °C –A Proof-of-Concept Study
TL;DR: Microwave-assisted organic synthesis in near-critical water (NCW) in the 270-300 °C temperature range has been investigated in a dedicated multimode microwave reactor utilizing heavy-walled quartz reaction vessels as discussed by the authors.
Book ChapterDOI
The Scale-Up of Microwave-Assisted Organic Synthesis
TL;DR: In this paper, the authors discuss several already known scale-up processes in microwave-assisted organic chemistry in a ≥50 mL batch scale and experiments performed with both continuous flow and stop-flow techniques.
Journal ArticleDOI
Microwaves in advanced oxidation processes for environmental applications. A brief review
TL;DR: In this paper, the influence of microwave radiation on photo assisted processes is discussed, and the possible advantages of microwaves in TiO2-assisted photodegradations and photomineralizations of various organic pollutants such as herbicides and endocrine disruptors.
References
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Journal ArticleDOI
Acceleration of the diels-alder reaction by aluminum chloride
Peter Yates,Philip E. Eaton +1 more
Journal ArticleDOI
Some Reactions of Δ2-Cyclohexenone, Including the Synthesis of Bicyclo(2,2,2)-octanedione-2,6
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The reaction of anthracene with maleic and fumaric acid and their derivatives and with citraconic anhydride and mesaconic acid.
W. E. Bachmann,L. B. Scott +1 more
TL;DR: The initial precipitate of long dense needles had become contaminated by a small superficial layer of fluffy crystalline balls, apparently containing the saturated dioltrione (XXIV) and after two further recrystallizations from alcohol melted at 23!-238’.
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Chlorination of organoboranes: synthesis of (z)-vinyl chlorides
TL;DR: Chloration d'(alcene-1yl dihydroxy) boranes et obtention stereoselective de cis-chloro-1 alcenes as mentioned in this paper.