Journal ArticleDOI
Application of commercial microwave ovens to organic synthesis.
TLDR
In this article, commercial microwave ovens have been safely used to dramatically reduce the reaction times (at comparable yield) of Diels-Alder, Claisen, and ene reactions.About:
This article is published in Tetrahedron Letters.The article was published on 1986-01-01. It has received 1028 citations till now. The article focuses on the topics: Microwave oven.read more
Citations
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Conversion of a non-water soluble potato starch waste into reducing sugars under non-conventional technologies
TL;DR: The comparison of the utilisation of different non-conventional technologies for the depolymerisation of a complex industrial starch-based waste into reducing sugars was investigated and it was found that reducing sugars could then be converted into higher value-added compounds such as higher alcohols.
Journal ArticleDOI
Continuous Flow Synthesis of Heterocycles: A Recent Update on the Flow Synthesis of Indoles.
TL;DR: The role of flow technology in the preparation of indole derivatives is showcased and selected examples have been described with the aim to provide readers with an overview on the tactics and technologies used for targeting indole scaffolds.
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An Efficient Procedure for the Synthesis of Spiro (3H-Indole-3,4′ (1′H)pyrano[2,3-C]pyrrole]-5′-carbonitriles Using Solid Inorganic Supports and Microwave Activation
TL;DR: In this article, 3-Dicyanoniethylene-2H-indol-2-one was synthesized under microwave irradiation using indole-2,3-dione and malononitrile.
Journal ArticleDOI
Heterogene Gasphasenkatalyse im Mikrowellenfeld
TL;DR: In this article, a review of microwave-assisted heterogeneous gas phase catalysis is presented, with a short introduction to the theory of dielectric heating, and hints to create more useful multimode microwave reactors are given.
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Microwave activation of catalysts and catalytic processes
Leonid M. Kustov,Ilya Sinev +1 more
TL;DR: In this paper, the results obtained by using microwave activation in catalytic processes such as the conversion of lower alkanes, the removal of volatile organic compounds and sulfur- and nitrogen-containing compounds from air, and the hydrogenation of aromatic compounds and dehydrogenation of naphthenes are discussed.
References
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Acceleration of the diels-alder reaction by aluminum chloride
Peter Yates,Philip E. Eaton +1 more
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Some Reactions of Δ2-Cyclohexenone, Including the Synthesis of Bicyclo(2,2,2)-octanedione-2,6
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The reaction of anthracene with maleic and fumaric acid and their derivatives and with citraconic anhydride and mesaconic acid.
W. E. Bachmann,L. B. Scott +1 more
TL;DR: The initial precipitate of long dense needles had become contaminated by a small superficial layer of fluffy crystalline balls, apparently containing the saturated dioltrione (XXIV) and after two further recrystallizations from alcohol melted at 23!-238’.
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Chlorination of organoboranes: synthesis of (z)-vinyl chlorides
TL;DR: Chloration d'(alcene-1yl dihydroxy) boranes et obtention stereoselective de cis-chloro-1 alcenes as mentioned in this paper.