Journal ArticleDOI
Application of commercial microwave ovens to organic synthesis.
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In this article, commercial microwave ovens have been safely used to dramatically reduce the reaction times (at comparable yield) of Diels-Alder, Claisen, and ene reactions.About:
This article is published in Tetrahedron Letters.The article was published on 1986-01-01. It has received 1028 citations till now. The article focuses on the topics: Microwave oven.read more
Citations
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Transition-Metal-Free Cross-Coupling of Aryl and N-Heteroaryl Cyanides with Benzylic Zinc Reagents
Pauline Quinio,Daniela Sustac Roman,Thierry León,Sharankini William,Konstantin Karaghiosoff,Paul Knochel +5 more
TL;DR: A novel oxidative nucleophilic substitution of a hydrogen on 1,3-dicyanobenzene using benzylic zinc reagents is reported, and selective benzylations on polycyano-aromatics have been achieved under mild conditions.
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Experimental study of a wearable aperture-coupled patch antenna for wireless body area network
TL;DR: In this paper, a new type of wearable aperture-coupled patch antenna for 2.4 GHz wireless body area network (WBAN) application is proposed, and the H-shaped slot in middle ground plane and rectangular ring microstrip feed line are optimized, so that it realizes the efficient electromagnetic coupling with the radiating element.
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Catalytic reactions enhanced under microwave-induced local thermal non-equilibrium in a core-shell, carbon-filled zeolite@zeolite
TL;DR: In this article, a core-shell, carbon-filled zeolite@zeolite was created through the epitaxial growth of shell zerosolite on a core zeolites filled with carbon.
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MW-assisted Er(OTf)3-catalyzed mild cleavage of isopropylidene acetals in Tricky substrates
TL;DR: Erbium(III) trifluoromethane sulfonate is proposed as a very gentle Lewis acid catalyst in a MW-assisted chemoselective method for the cleavage of isopropylidene acetals in awkward substrates by using pure water as the solvent as discussed by the authors.
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Microwaves and their coupling to advanced oxidation processes: enhanced performance in pollutants degradation.
TL;DR: Based on the results surveyed in the literature, MW/AOPs are promising alternatives for treating/remediating environmental pollutants, whenever one considers high degradation yields, short reaction times, and small costs.
References
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Journal ArticleDOI
Acceleration of the diels-alder reaction by aluminum chloride
Peter Yates,Philip E. Eaton +1 more
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Some Reactions of Δ2-Cyclohexenone, Including the Synthesis of Bicyclo(2,2,2)-octanedione-2,6
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The reaction of anthracene with maleic and fumaric acid and their derivatives and with citraconic anhydride and mesaconic acid.
W. E. Bachmann,L. B. Scott +1 more
TL;DR: The initial precipitate of long dense needles had become contaminated by a small superficial layer of fluffy crystalline balls, apparently containing the saturated dioltrione (XXIV) and after two further recrystallizations from alcohol melted at 23!-238’.
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Chlorination of organoboranes: synthesis of (z)-vinyl chlorides
TL;DR: Chloration d'(alcene-1yl dihydroxy) boranes et obtention stereoselective de cis-chloro-1 alcenes as mentioned in this paper.