Journal ArticleDOI
Application of commercial microwave ovens to organic synthesis.
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In this article, commercial microwave ovens have been safely used to dramatically reduce the reaction times (at comparable yield) of Diels-Alder, Claisen, and ene reactions.About:
This article is published in Tetrahedron Letters.The article was published on 1986-01-01. It has received 1028 citations till now. The article focuses on the topics: Microwave oven.read more
Citations
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Microwave-assisted synthesis of calcium carbonate (vaterite) of various morphologies in water-ethylene glycol mixed solvents.
Rui-Juan Qi,Ying-Jie Zhu +1 more
TL;DR: The experiments show that microwave heating, reaction time, surfactant, and the water-EG mixed solvents play important roles in the morphology of vaterite.
Journal ArticleDOI
Photochemistry with microwaves: Catalysts and environmental applications
Satoshi Horikoshi,Nick Serpone +1 more
TL;DR: In this article, the role of microwave radiation has been examined not only as a dielectric heat source but also a source of vacuum-UV radiation and UV light through microwave discharge electrodeless lamp devices, which in some cases can also serve as photoreactors.
Journal ArticleDOI
Enzymatic modification of cassava starch by fungal lipase
TL;DR: In this article, starch esterification was carried out to expand the usefulness of starch for a myriad of industrial applications, including plastic industry, pharmaceutical industry, and biomedical applications such as materials for bone fixation and replacements, carriers for controlled release of drugs and other bioactive agents.
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High temperature metalation of functionalized aromatics and heteroaromatics using (tmp)2Zn x 2 MgCl2 x 2 LiCl and microwave irradiation.
TL;DR: A wide range of polyfunctional aryl and heteroaryl zinc reagents were efficiently prepared in THF via direct zincation using (tmp)2Zn x 2 MgCl2 x 2 LiCl and microwave irradiation, leading to highly functionalized aromatics andheteroaromatics in good to excellent yields.
Journal ArticleDOI
Microwave‐Hydrothermal Processing of BiFeO3 and CsAl2PO6
TL;DR: In this article, the authors compared microwave-hydrothermal (M-H) processing with conventional H-H processing in the crystallization of BiFeO3 and CsAl2PO6 phases.
References
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Journal ArticleDOI
Acceleration of the diels-alder reaction by aluminum chloride
Peter Yates,Philip E. Eaton +1 more
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Some Reactions of Δ2-Cyclohexenone, Including the Synthesis of Bicyclo(2,2,2)-octanedione-2,6
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The reaction of anthracene with maleic and fumaric acid and their derivatives and with citraconic anhydride and mesaconic acid.
W. E. Bachmann,L. B. Scott +1 more
TL;DR: The initial precipitate of long dense needles had become contaminated by a small superficial layer of fluffy crystalline balls, apparently containing the saturated dioltrione (XXIV) and after two further recrystallizations from alcohol melted at 23!-238’.
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Chlorination of organoboranes: synthesis of (z)-vinyl chlorides
TL;DR: Chloration d'(alcene-1yl dihydroxy) boranes et obtention stereoselective de cis-chloro-1 alcenes as mentioned in this paper.