Journal ArticleDOI
Application of commercial microwave ovens to organic synthesis.
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In this article, commercial microwave ovens have been safely used to dramatically reduce the reaction times (at comparable yield) of Diels-Alder, Claisen, and ene reactions.About:
This article is published in Tetrahedron Letters.The article was published on 1986-01-01. It has received 1028 citations till now. The article focuses on the topics: Microwave oven.read more
Citations
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Regeneration of carbonyl compounds from oximes, hydrazones, semicarbazones, acetals, 1,1-diacetates, 1,3-dithiolanes, 1,3-dithianes and 1,3-oxathiolanes
TL;DR: In this article, the authors proposed a method of deoximation with organic reagents and supported reagents under Microwave Irradiation (MIR) under microwave radiation.
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Versatile access to benzhydryl-phenylureas through an unexpected rearrangement during microwave-enhanced synthesis of hydantoins.
Giulio G. Muccioli,Johan Wouters,Jacques H. Poupaert,Bernadette Norberg,Wolfgang Poppitz,Gerhard K. E. Scriba,Didier M. Lambert +6 more
TL;DR: This new reaction proved to be an easy access to substituted 1-benzhydryl-3-phenyl-ureas, demonstrating that only phenylurea derivatives can result in benzhydryL- Phenylureas under the applied conditions.
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Stereoselective glycosylation of exo-glycals by microwave-assisted Ferrier rearrangement
TL;DR: Interestingly exo -glycals were found to have higher activity than endo - glycals and common glycosides, the reactions of which can be improved by the addition of Lewis acid to result in a higher yield and enhanced stereoselectivity.
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Surface-Mediated Synthesis of O-Alkyl 2-Methoxyethyl Alkylphosphonates Under Solvent Free Conditions: Potential Marker of Nerve Agents
TL;DR: In this paper, a surface mediated synthesis of O-alkyl 2-methoxyethyl alkylphosphonates (AMEAPs) using DCC-Celite as a solid support is described.
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Microwave-assisted Functionalization of Carbon Nanostructured Materials
TL;DR: An overview of microwave-assisted functionalization of carbon nanostructured materials is presented in this article, covering major breakthroughs achieved in the last years for this novel, intriguing and non-conventional synthetic approach.
References
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Journal ArticleDOI
Acceleration of the diels-alder reaction by aluminum chloride
Peter Yates,Philip E. Eaton +1 more
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Some Reactions of Δ2-Cyclohexenone, Including the Synthesis of Bicyclo(2,2,2)-octanedione-2,6
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The reaction of anthracene with maleic and fumaric acid and their derivatives and with citraconic anhydride and mesaconic acid.
W. E. Bachmann,L. B. Scott +1 more
TL;DR: The initial precipitate of long dense needles had become contaminated by a small superficial layer of fluffy crystalline balls, apparently containing the saturated dioltrione (XXIV) and after two further recrystallizations from alcohol melted at 23!-238’.
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Chlorination of organoboranes: synthesis of (z)-vinyl chlorides
TL;DR: Chloration d'(alcene-1yl dihydroxy) boranes et obtention stereoselective de cis-chloro-1 alcenes as mentioned in this paper.