Journal ArticleDOI
Application of commercial microwave ovens to organic synthesis.
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In this article, commercial microwave ovens have been safely used to dramatically reduce the reaction times (at comparable yield) of Diels-Alder, Claisen, and ene reactions.About:
This article is published in Tetrahedron Letters.The article was published on 1986-01-01. It has received 1028 citations till now. The article focuses on the topics: Microwave oven.read more
Citations
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Journal ArticleDOI
Unexpected synthesis of N-methylbenzo[d]isoxazolium hydroxides under microwave irradiation conditions.
TL;DR: Microwave-assisted condensation of salicylaldehydes and N-methyl hydroxylammonium hydrochloride in the presence of K2CO3 under solvent-free conditions afforded, unexpected N- methylbenzo[d]isoxazolium hydroxides (2a–d).
Journal ArticleDOI
MAOS of Quinoxalines, Conjugated Pyrazolylquinoxalines and Fused Pyrazoloquinoxalines from l‐Ascorbic and d‐Isoascorbic Acid
TL;DR: In this paper, microwave assisted organic synthesis (MAOS) has been used to accelerate the conversion of Lascorbic acid (1) and Discorbic acids (2) to the title heterocycles by conversion to 3.
Book ChapterDOI
Hydrothermal Technology for Nanotechnology—A Technology for Processing of Advanced Materials
TL;DR: An overview of the current trends in materials processing, the new concepts emerging out in recent years and the future trends in hydrothermal research is provided in this paper, with suitable examples of fine particles, ultra-fine particles and nanoparticles.
Journal ArticleDOI
Improving methodology for the preparation of uracil derivatives from Fischer carbene complexes. Microwave activation
TL;DR: In this article, the effect of microwave irradiation on the reaction of alkynyl alkoxy carbene complexes with ureas was studied and it was shown that the use of microwave activation could represent an alternative to the reaction in conventional conditions for the metal carbene complex chemistry.
Journal ArticleDOI
Current perspectives on microwave-enhanced reactions of monosaccharides promoted by heterogeneous catalysts
TL;DR: In this article, the use of ion exchange resins, zeolites, clays and metal oxides as convenient mediators for key transformations of carbohydrates is discussed, and a special emphasis is placed on use of (doped) mineral supports, in solventless conditions, as clean promoters in combination with microwave dielectric heating.
References
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Journal ArticleDOI
Acceleration of the diels-alder reaction by aluminum chloride
Peter Yates,Philip E. Eaton +1 more
Journal ArticleDOI
Some Reactions of Δ2-Cyclohexenone, Including the Synthesis of Bicyclo(2,2,2)-octanedione-2,6
Journal ArticleDOI
The reaction of anthracene with maleic and fumaric acid and their derivatives and with citraconic anhydride and mesaconic acid.
W. E. Bachmann,L. B. Scott +1 more
TL;DR: The initial precipitate of long dense needles had become contaminated by a small superficial layer of fluffy crystalline balls, apparently containing the saturated dioltrione (XXIV) and after two further recrystallizations from alcohol melted at 23!-238’.
Journal ArticleDOI
Chlorination of organoboranes: synthesis of (z)-vinyl chlorides
TL;DR: Chloration d'(alcene-1yl dihydroxy) boranes et obtention stereoselective de cis-chloro-1 alcenes as mentioned in this paper.