Journal ArticleDOI
Application of commercial microwave ovens to organic synthesis.
TLDR
In this article, commercial microwave ovens have been safely used to dramatically reduce the reaction times (at comparable yield) of Diels-Alder, Claisen, and ene reactions.About:
This article is published in Tetrahedron Letters.The article was published on 1986-01-01. It has received 1028 citations till now. The article focuses on the topics: Microwave oven.read more
Citations
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Worm-like mesoporous structured iron-based fluoride: Facile preparation and application as cathodes for rechargeable lithium ion batteries
TL;DR: In this article, a worm-like mesoporous structured iron-based fluoride (Fe 1.9 F 4.75 · 0.95H 2 O) was successfully synthesized for the first time by a rapid microwave irradiation heating route using ionic liquid 1-butyl-3-methylimidazolium tetrafluoroborate (BmimBF 4 ) as fluorine source and iron (III) nitrate nonahydrate (Fe(NO 3 ) 3 ·9H 2O) as iron source.
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A new and original microwave continuous reactor under high pressure for future chemistry
TL;DR: In this paper, a new high pressure reactor for continuous flow chemistry under microwaves at industrial scale was designed and developed, which allows continuous chemical reactions at a kg/h scale, under microwave heating, up to 7 MPa and 200°C.
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The effect of microwave energy on specific migration from food contact plastics.
TL;DR: Experiments have been carried out with microwave treatment of plastics followed by migration testing using the food simulant, olive oil, and in neither of these complementary approaches was there evidence of any difference in migration from plastics that have been microwave-treated compared with plastics that had received an equivalent thermal treatment.
Journal ArticleDOI
Efficient and Selective Protection of Alcohols and Phenols with Triisopropylsilyl Chloride/Imidazole Using Microwave Irradiation
TL;DR: In this article, a simple and efficient method was described for silylation of alcohols and phenols using triisopropylsilyl chloride and imidazole under microwave irradiation.
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Improved synthesis of 3-spiro indolines in dry media under microwave irradiation
TL;DR: In this paper, an efficient one-pot synthesis of spiro [indole-dipyrrolopyrylopyridines] was achieved under microwave irradiation by the interaction with ammonium acetate (7) in the presence of acetic acid.
References
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Journal ArticleDOI
Acceleration of the diels-alder reaction by aluminum chloride
Peter Yates,Philip E. Eaton +1 more
Journal ArticleDOI
Some Reactions of Δ2-Cyclohexenone, Including the Synthesis of Bicyclo(2,2,2)-octanedione-2,6
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The reaction of anthracene with maleic and fumaric acid and their derivatives and with citraconic anhydride and mesaconic acid.
W. E. Bachmann,L. B. Scott +1 more
TL;DR: The initial precipitate of long dense needles had become contaminated by a small superficial layer of fluffy crystalline balls, apparently containing the saturated dioltrione (XXIV) and after two further recrystallizations from alcohol melted at 23!-238’.
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Chlorination of organoboranes: synthesis of (z)-vinyl chlorides
TL;DR: Chloration d'(alcene-1yl dihydroxy) boranes et obtention stereoselective de cis-chloro-1 alcenes as mentioned in this paper.