Journal ArticleDOI
Application of commercial microwave ovens to organic synthesis.
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In this article, commercial microwave ovens have been safely used to dramatically reduce the reaction times (at comparable yield) of Diels-Alder, Claisen, and ene reactions.About:
This article is published in Tetrahedron Letters.The article was published on 1986-01-01. It has received 1028 citations till now. The article focuses on the topics: Microwave oven.read more
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Understanding MAOS through computational chemistry
TL;DR: This review provides an overview of the use of Computational Chemistry inMAOS to provide a theoretical understanding of the factors that can be used to explain the improvements in MAOS and how computational calculations can be use as a predictive tool.
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Microwave sintering, characterization and magnetic properties of double perovskite La2CoMnO6 nanoparticles
TL;DR: Double perovskite La2CoMnO6 (LCMO) nanoparticles were successfully synthesized by a convenient, environmentally friendly, inexpensive and efficient chemical co-precipitation process and subsequently sintered at 900 degrees C/10 min using microwave sintering (MW) for the first time as mentioned in this paper.
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Rapid Synthesis of Aromatic Polyamides by Microwave-Assisted Directed Polycondensation of Aromatic Diamines with Aromatic Dicarboxilic Acids
TL;DR: Rapid Synthesis of Aromatic Polyamides by Microwave-Assisted Directed Polycondensation of aromatic Diamines with Aromatically Dicarboxilic Acids as discussed by the authors.
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Microwave and continuous flow technologies in drug discovery
TL;DR: Microwave and continuous flow microreactors have become mainstream heating sources in contemporary pharmaceutical company laboratories, and the combined force of these technologies offers the potential to revolutionize discovery and manufacturing processes.
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Synthesis of pyrazolo[1,5-a]pyrimidine derivatives and their antifungal activities against phytopathogenic fungi in vitro.
TL;DR: The antifungal properties of 3 and 4 were tested against Cytospora sp.
References
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Journal ArticleDOI
Acceleration of the diels-alder reaction by aluminum chloride
Peter Yates,Philip E. Eaton +1 more
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Some Reactions of Δ2-Cyclohexenone, Including the Synthesis of Bicyclo(2,2,2)-octanedione-2,6
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The reaction of anthracene with maleic and fumaric acid and their derivatives and with citraconic anhydride and mesaconic acid.
W. E. Bachmann,L. B. Scott +1 more
TL;DR: The initial precipitate of long dense needles had become contaminated by a small superficial layer of fluffy crystalline balls, apparently containing the saturated dioltrione (XXIV) and after two further recrystallizations from alcohol melted at 23!-238’.
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Chlorination of organoboranes: synthesis of (z)-vinyl chlorides
TL;DR: Chloration d'(alcene-1yl dihydroxy) boranes et obtention stereoselective de cis-chloro-1 alcenes as mentioned in this paper.