Journal ArticleDOI
Application of commercial microwave ovens to organic synthesis.
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In this article, commercial microwave ovens have been safely used to dramatically reduce the reaction times (at comparable yield) of Diels-Alder, Claisen, and ene reactions.About:
This article is published in Tetrahedron Letters.The article was published on 1986-01-01. It has received 1028 citations till now. The article focuses on the topics: Microwave oven.read more
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General areas of the use of a microwave radiation for processing of plant raw materials (review)
TL;DR: The use of microwave radiation in the chemistry of plant raw materials has attracted the attention of a growing number of scientists as mentioned in this paper, including extraction of low-molecular weight compounds of different classes both in an individual state and in compositions (for example, essential oils) from natural plant objects.
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Microwave assisted slurry conversion crystallization for manufacturing of new co-crystals of sulfamethazine and sulfamerazine
Dipali Ahuja,Kiran A. Ramisetty,Peraka Krishna Sumanth,C. M. Crowley,Matteo Lusi,Åke C. Rasmuson +5 more
TL;DR: In this paper, two sulfa drugs, sulfamethazine and sulfamerazine, have been used as model compounds in the evaluation of microwave assisted slurry conversion crystallization for manufacturing of co-crystals.
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Solvent free synthesis, crystal studies, docking studies and antibacterial properties of some novel fluorinated pyridazinone derivatives
H.B.V. Sowmya,T.H. Suresha Kumara,T.H. Suresha Kumara,Gopalpur Nagendrappa,Jerry P. Jasinski,Sean P. Millikan,Gilish Jose,R. Dileep,P. S. Sujan Ganapathy +8 more
TL;DR: The solvent free synthesis of six 6-(3,5-difluorophenyl)-4,5dihydropyridazin-3(2 H )-one derivatives was carried out by microwave irradiation of a pulverized mixture of 4-oxobutanoic acid and substituted hydrazine hydrochloride in presence of catalytic amount of acetic acid at 150°C/75 W for 5min this article.
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Microwave Assisted Synthesis of Monoazanaphthalene Scaffolds
TL;DR: A review of microwave assisted synthesis of quinoline and isoquinoline can be found in this paper, where the authors discuss the current achievements in microwave-assisted synthesis of these compounds.
References
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Journal ArticleDOI
Acceleration of the diels-alder reaction by aluminum chloride
Peter Yates,Philip E. Eaton +1 more
Journal ArticleDOI
Some Reactions of Δ2-Cyclohexenone, Including the Synthesis of Bicyclo(2,2,2)-octanedione-2,6
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The reaction of anthracene with maleic and fumaric acid and their derivatives and with citraconic anhydride and mesaconic acid.
W. E. Bachmann,L. B. Scott +1 more
TL;DR: The initial precipitate of long dense needles had become contaminated by a small superficial layer of fluffy crystalline balls, apparently containing the saturated dioltrione (XXIV) and after two further recrystallizations from alcohol melted at 23!-238’.
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Chlorination of organoboranes: synthesis of (z)-vinyl chlorides
TL;DR: Chloration d'(alcene-1yl dihydroxy) boranes et obtention stereoselective de cis-chloro-1 alcenes as mentioned in this paper.